An automated distillation method for the determination of diacetyl in beer: a comparison of analysis by AutoAnalyzer and gas chromatography
1979

Automated Method for Measuring Diacetyl in Beer

Sample size: 25 publication Evidence: high

Author Information

Author(s): J. C. Buijten, B. Holm

Primary Institution: Department of Alcohol and Drug Addiction Research, Karolinska Institutet

Hypothesis

The aim of the work described in this paper was to develop a fully automated method for the colorimetric determination of diacetyl in beer using a Technicon AutoAnalyzer II system.

Conclusion

The automated method for measuring diacetyl in beer showed a high correlation with gas chromatography results.

Supporting Evidence

  • The correlation between the automated method and gas chromatography was highly significant, with R = 0.996.
  • The precision of the AutoAnalyzer method was repeatable to + 3.170.
  • The distillation step was identified as the most critical stage in the determination of diacetyl.

Takeaway

This study created a machine that can quickly and accurately measure a chemical in beer that affects its taste.

Methodology

The study used an automated distillation method coupled with a Technicon AutoAnalyzer II to measure diacetyl in beer samples.

Limitations

The study noted that prolonged distillation and high temperatures could lead to inaccurate results.

Statistical Information

P-Value

< 0.001

Statistical Significance

p<0.001

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