Synthesis of diverse dihydropyrimidine-related scaffolds by fluorous benzaldehyde-based Biginelli reaction and post-condensation modifications
2011

Synthesis of Dihydropyrimidine Compounds

publication Evidence: moderate

Author Information

Author(s): Piqani Bruno, Zhang Wei, Müller Thomas J

Primary Institution: University of Massachusetts Boston

Hypothesis

The study investigates the efficiency of a diversity-oriented synthesis of dihydropyrimidine-related compounds using fluorous benzaldehyde-based Biginelli reactions.

Conclusion

The study successfully developed a new application of fluorous benzaldehydes for synthesizing diverse heterocyclic scaffolds with high efficiency.

Supporting Evidence

  • The Biginelli reaction is an efficient method for synthesizing dihydropyrimidinones.
  • Microwave heating significantly speeds up the reaction process.
  • Fluorous solid-phase extractions simplify the purification of the products.

Takeaway

The researchers found a new way to make different chemical compounds quickly and easily using special ingredients and techniques.

Methodology

The study utilized a Biginelli reaction followed by post-condensation modifications under microwave heating and fluorous solid-phase extractions.

Digital Object Identifier (DOI)

10.3762/bjoc.7.150

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